Microscopy Electron
Mostrando 1-12 de 9551 artigos, teses e dissertações.
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1. Study of rhombohedral tricalcium phosphate in hexagonal crystal structure family on the sample prepared by the sol-gel route and the effect of calcination temperature
Abstract The effect of the calcination temperature at 800 and 1000 °C on the stable formation of the tricalcium phosphate with rhombohedral structure in the system of the hexagonal crystal family was determined, while its precursor was made from limestone obtained from nature in the Lumajang district, Indonesia. The rhombohedral tricalcium phosphate samples
Cerâmica. Publicado em: 2023
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2. Synthesis of delafossite CuCrO2 via solution combustion method and its acid functionalization for biodiesel production
Abstract CuCrO2 was synthesized by solution combustion synthesis (SCS) and applied as a heterogeneous catalyst to produce soybean biodiesel. The combustion reaction was carried out using urea as a fuel, and copper (II) and chromium (III) nitrates as precursors. After the powders’ obtention, these were calcined and functionalized in an acidic medium. The po
Cerâmica. Publicado em: 2023
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3. Carbon Dots from Pilosocereus gounellei for Fluorimetric Determination of Tannin in Tea Using a Flow-Batch System
In this study, xiquexique (Pilosocereus gounellei) native endemic cactus from the Brazilian semiarid was used for the first time as a natural carbon source (“green precursor”) for the synthesis of highly fluorescent carbon dots (CDs). These CDs were successfully used to develop a fast, low-cost, eco-friendly fluorescence method for the determination of t
Journal of the Brazilian Chemical Society. Publicado em: 2023
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4. The influence of compositional variability of dimension stone residues on the properties of rustic porous ceramic tiles
Abstract This study analyzed how the compositional variability of dimension stone residues influences the characteristics of rustic porous ceramic tiles. The specimens were prepared by adding 20 wt% of dimension stone residue to the clay and sintered at 1000 °C for 1 h. The testing assays performed were physical properties and structural analysis through sc
Cerâmica. Publicado em: 2023
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5. McCune-Albright syndrome - A case report with transmission electron microscopy
Abstract McCune - Albright syndrome is a genetic disease with cutaneous mosaicism caused by post-zygotic activating mutations in GNAS locus, it has a triad of fibrous bone dysplasia, café-au-lait macules and precocious puberty. We examined a 22-year-old female patient with café au lait spot in right side of the abdomen, with a chessboard - like distributio
Anais Brasileiros de Dermatologia. Publicado em: 2022
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6. Transmission electron microscopy of pili annulati
Abstract Background: Little is known about the ultrastructure of pili annulati. Objectives: To examine with transmission electron microscopy affected hairs of a family, whose diagnosis had been confirmed in five individuals with scanning electron microscopy, which showed surface undulations with ‘‘curtain-like’’ folding of the hair cuticula and to
Anais Brasileiros de Dermatologia. Publicado em: 2022
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7. Study of nanocomposites with carbon nanotubes and their tendency for carbon organization
Abstract The carbon derived from the thermal treatment of modified phenolic resins (PR) tends to organize into graphitic lamellae or turbostratic carbon and is commonly considered non-graphitizable. In this study, nanocomposites were synthesized with modified phenolic resin (Novolac) used as the matrix and oxidized multi-walled carbon nanotubes (NTox) in amo
Cerâmica. Publicado em: 2022
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8. Scanning electron microscopy of panitumumab-induced eyelash and hair alterations - Pili canaliculi
Abstract Panitumumab is a monoclonal antibody against the epidermal growth factor receptor used in metastatic colorectal cancer; in addition to tumor cells, it acts on epidermal keratinocytes and on the outer root sheath and presents skin toxicity in up to 90% of cases. A scanning electron microscope was used to examine the eyelashes and hairs of a 65-year-o
Anais Brasileiros de Dermatologia. Publicado em: 2022
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9. X-ray line profile analysis and magnetic and optical properties of FexZn0.95-xCr0.05O nanoparticles fabricated by sol-gel route
Abstract FexZn0.95-xCr0.05O nanoparticles have been obtained for the different concentrations of Fe ions by using the sol-gel method. The hexagonal wurtzite structure of all the samples was confirmed by Rietveld refined X-ray diffraction patterns. The addition of Fe ions decreased lattice constants a and c from 3.2487 to 3.2474 Å and 5.2043 to 5.2029 Å, re
Cerâmica. Publicado em: 2022
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10. Graphite-Polyurethane Composite Electrode Modified with Molecularly Imprinted Polymer for Determination of Diclofenac
A molecularly imprinted polymer (MIP) was prepared using the anti-inflammatory diclofenac (DCF) as a template. A non-imprinted polymer (NIP) was also prepared as a control. These MIP and NIP were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Brunauer-Emmett-Teller (BET), revealing a higher porosity in the fir
Journal of the Brazilian Chemical Society. Publicado em: 2022
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11. Characterization of micaceous minerals occurring in phosphate ores in Brazil: emphasis on the interstratified phyllosilicates
Abstract Micaceous minerals were characterized in three phosphatic ores from mines in Western Minas Gerais State, Brazil, all having complex chemical and mineralogical compositions, with emphasis on interstratified phyllosilicates. Knowledge of the relationship between the physical and chemical characteristics of the phyllosilicates contributed to a better u
REM - International Engineering Journal. Publicado em: 2022
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12. Morphology Behavior of Copper Films Deposited after Wet Surface Treatment on Polished Alumina
In this paper, a pre-treatment process for electroless copper (Cu) deposition on the polished alumina (Al2O3) 99.9% and the behavior of Cu plating by electroless process after Al2O3 surface treatment were explored. Our work was carried out by changing the roughness of Al2O3 through micro-etching (coarsening), nucleation its surface by a two-step method (sens
Journal of the Brazilian Chemical Society. Publicado em: 2022