Thermal Analysis And Chromatographic
Mostrando 1-12 de 24 artigos, teses e dissertações.
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1. Development and Validation of a Gas Chromatographic Method for the Quantification of Minor Alkaloids in Cocaine
The quantification of minor alkaloids in seized cocaine can provide information for drug profiling and law enforcement initiatives. This work presents the development and validation of an analytical method to quantitate minor alkaloids in cocaine samples using gas chromatography with flame ionization detector, after derivatization. The method was validated i
J. Braz. Chem. Soc.. Publicado em: 2021-04
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2. Blue Glow Sticks: Cinnamic Acids and Arylacrylonitriles with Liquid-Crystalline Properties and Highly Fluorescent
Five new π-conjugated chromophores derived from acrylic acid and acrylonitrile were synthesized and their thermal and photophysical behaviors were analyzed. They were designed and synthesized through Knoevenagel condensations between arylacetylenebenzaldehydes and a methylene group activated from cyanoacetic and malonic acids. The characterization of the ta
J. Braz. Chem. Soc.. Publicado em: 2021-01
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3. Evaluation of quality parameters and chromatographic, spectroscopic, and thermogravimetric profile of Patauá oil (Oenocarpus bataua)
Abstract The objective of this research was to evaluate the quality parameters and the chromatographic, thermogravimetric, and spectroscopic profile of Patauá oil (Oenocarpus bataua). All analyses were performed according to the Recommended Practices of the American Oil Chemists’ Society (AOCS). The parameters obtained indicate conservation quality standa
Food Sci. Technol. Publicado em: 2020-06
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4. Evaluation of quality parameters and chromatographic, spectroscopic, and thermogravimetric profile of Patauá oil (Oenocarpus bataua)
Abstract The objective of this research was to evaluate the quality parameters and the chromatographic, thermogravimetric, and spectroscopic profile of Patauá oil (Oenocarpus bataua). All analyses were performed according to the Recommended Practices of the American Oil Chemists’ Society (AOCS). The parameters obtained indicate conservation quality standa
Food Sci. Technol. Publicado em: 09/09/2019
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5. FOURIER TRANSFORM INFRARED SPECTROSCOPY, THERMOGRAVIMETRIC ANALYSIS, SCANNING ELECTRON MICROSCOPY AS SUPPORTING TOOLS IN QUALITY CONTROL OF ANTIPARASITICS
This study shows that Fourier transform infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), and scanning electron microscopy (SEM) can be used as supporting tools for the evaluation of the quality of antiparasitics. In addition, an analytical methodology was developed and validated to quantify simultaneously thiabendazole (TB), febantel (FB), tol
Quím. Nova. Publicado em: 2018-03
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6. Thermal degradation kinetics of ascorbic acid, thiamine and riboflavin in rosehip (Rosa canina L) nectar
Abstract In this paper, the loss of L-ascorbic acid, thiamine and riboflavin in rosehip nectar with the heating periods (0, 5, 10, 15, 20 and 30 min) at temperatures ranging from 70 to 95 °C is analyzed and experimental results are presented. Firstly, dried rosehip fruits were processed to rosehip nectar and then thermal treatment is performed. Liquid chrom
Food Sci. Technol. Publicado em: 19/10/2017
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7. AvaliaÃÃo do desempenho de ligante asfÃltico modificado por poli (Ãcido fosfÃrico) (PPA) e efeitos da adiÃÃo do lÃquido da casca da castanha de caju (LCC). / Performance evaluation of asphalt binder modified poly (phosphoric acid) (PPA) and effects adding the liquid from the bark of cashew (LCC)
The AC with 50/70 penetration grade (Petrobras - LUBNOR), pure and modified by polyphosphoric acid (PPA), was analyzed by rheological tests (viscosity and DSR), thermal analysis (TGA and DSC), spectrometric (NMR and FTIR) and chromatographic (TLC-FID and GPC) methods. The interaction of AC with PPA was investigated from the reactions of its fractions (aromat
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 09/12/2011
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8. DEPLOYMENT OF METHOD FOR ANALYSIS OF STABLE CARBON ISOTOPES (N-ALKANES C1-C5) IN GAS SAMPLES AT LOW CONCENTRATIONS / IMPLANTAÇÃO DE MÉTODO PARA ANÁLISE DE ISÓTOPOS ESTÁVEIS DE CARBONO (N-ALCANOS C1-C5) EM GASES A BAIXAS CONCENTRAÇÕES
The concentration and isotopic composition of n-alkanes C1-C5 has revealed as a powerful tool for interpretation of interesting processes in the oil exploration industry, studies of global climate change, oil biodegradation and carbon cycle elucidation. In this context, studies about methane analysis have been distinguished and multiplied due to the importan
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 06/10/2011
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9. Desenvolvimento de método químico analítico forense para análise de merla por Análise Térmica e Cromatografia Gasosa de Alta Resolução / Development of forensic analytical chemistry method for examination of merla by Thermal Analysis and High Resolution Gas chromatography
Neste estudo realizou-se o desenvolvimento de um método químico analítico forense para a análise de uma droga ilícita a base de cocaína, a merla. As análises termogravimétricas permitiram conhecer o comportamento térmico das amostras e quantificar as etapas de perdas de massa, que juntamente com a quantificação de evento endotérmico em DSC, foram
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 18/03/2011
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10. Synthesis, characterization and catalytic activity of mesoporous materials Al-MCM-41 in transesterification reaction of cottonseed oil / Síntese, caracterização e avaliação catalítica do aluminossilicato mesoestruturado AI-MCM-41 na transesterificação de óleos vegetais
Molecular sieves have been applied to the processing of triacylglycerols, to produce biofuels. In this context, the mesoporous catalyst Al-MCM-41 was proposed in this work as an alternative to acid heterogeneous transesterification of cottonseed oil with ethanol. This material was prepared using various Si/Al molar ratios (25, 50, 75 and 100) with reaction t
Publicado em: 2010
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11. Production and characterization of the biofuels by cracking of vegetable oils through bauxite catalysis / Produção e Caracterização de Biocombustíveis por Craqueamento de Óleo Vegetais via Catálise com Bauxita
In this work, raw bauxite, thermally activated calcined bauxite, calcined bauxite underwent acid treatment were the catalysts tested by its potential in the thermal catalytic cracking reaction looking forward to the production of biofuels from commercial soybean oil as an alternative to fossil fuels. The materials were characterized by the techniques ICP-OES
Publicado em: 2009
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12. Produção e Caracterização de Biocombustíveis por Craqueamento de Óleo Vegetais via Catálise com Bauxita / Production and characterization of the biofuels by cracking of vegetable oils through bauxite catalysis
In this work, raw bauxite, thermally activated calcined bauxite, calcined bauxite underwent acid treatment were the catalysts tested by its potential in the thermal catalytic cracking reaction looking forward to the production of biofuels from commercial soybean oil as an alternative to fossil fuels. The materials were characterized by the techniques ICP-OES
Publicado em: 2009