Scanning Electronic Microscopy
Mostrando 1-12 de 234 artigos, teses e dissertações.
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1. EFFECT OF REACTION CONDITIONS ON PARTICLE SIZE OF ZNO NANOPARTICLES VIA CONTROLLED PRECIPITATION METHOD AND IN-VITRO ANTIBACTERIAL CAPACITY
High-yield ZnO spheroidal nanoparticles with an average diameter around 23 nm (≈ 25% frequency) and 30 nm (≈ 28% frequency) were obtained by controlled semicontinuous precipitation at low temperatures. This synthesis was obtained from hydrozincite (Zn5(CO3)2(OH)6) as primary nanoparticles. The Zn5(CO3)2(OH)6 nanoparticles were synthesized by hydrolysis o
Química Nova. Publicado em: 2022
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2. Designing and fabrication of a low-cost dip-coater for rapid production of uniform thin films
In this work, a self-made dip-coater equipment was developed for the fabrication of thin films. The assembly of the apparatus was carried out using simple mechanical and electronic pieces, recycle parts, and spending an inexpensive budget suitably. The production, software design, and features of the device were focused on the sol-gel dip-coating method, whi
Química Nova. Publicado em: 2022
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3. ERRATUM
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Arq. Neuro-Psiquiatr.. Publicado em: 2021-06
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4. Polyamide 11 porous films by NIPS: the influence of miscibility and polymer crystalline formation in pores structure and morphology
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Quím. Nova. Publicado em: 2021-06
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5. Heterotopic Heart Transplant History and Concepts Cannot Be Neglected - Witnessing the History and Learning with Previous Practices
This study described the morphology, crystallinity, thermal and mechanical characterization of Polyamide 11 (PA11) porous film prepared by non-solvent induced phase separation (NIPS) method using formic acid (FA) as solvent. In addition, the miscibility of PA11/FA/H2O system was performed to generate a ternary phase diagram. The porous films morphology was i
Braz. J. Cardiovasc. Surg.. Publicado em: 2021-06
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6. Calcium oxalate content from two Amazonian amilaceous roots and the functional properties of their isolated starches
Abstract The calcium oxalate content from two Amazonian amilaceous roots, Xanthosoma sagittifolium and Pachyrhizus tuberosus, before and after cooking were studied in the present work. Calcium oxalate raphides were observed by light microscopy in longitudinal sections from fresh tubers. The functional properties and physicochemical characteristics of isolate
Food Sci. Technol. Publicado em: 2020-09
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7. Effect of Solid Solution Temperature on Microstructure and Corrosion Resistance of CoNiCrMo Alloy
Influence of solid solution temperature on microstructures and corrosion properties of CoNiCrMo alloy were investigated by means of optical microscopy (OM), scanning electron microscope (SEM) and electronic differential system. The corrosion resistance of CoNiCrMo alloy in 0.9%NaCl aqueous solution was also investigated. The results indicated that with the i
Mat. Res.. Publicado em: 24/10/2019
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8. Glass fiber post treatment – does it influence resin cement bond strength?
Resumo Introdução Pinos de fibra de vidro são utilizados para melhorar a retenção das restaurações em dentes tratados endodonticamente. Objetivo Avaliar a resistência de união de pinos de fibra de vidro submetidos a diferentes tratamentos superficiais e cimentados à dentina radicular com cimento resinoso autoadesivo. Material e método trinta ra
Rev. odontol. UNESP. Publicado em: 26/09/2019
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9. Influência da adição de Sn na resistência à corrosão e na capacidade de recarga da liga Pb-1,5%Sn para grade positiva de baterias chumbo-ácido
RESUMO O presente trabalho teve como objetivo avaliar o processo de corrosão do Pb e da liga Pb-1,5%Sn quando submetidos à condição de ciclagem em meio de ácido sulfúrico, visando compreender a influência da adição de Sn na resistência à corrosão e na capacidade de recarga para grades positivas de baterias do Pb-ácido. As amostras de estudo fora
Matéria (Rio J.). Publicado em: 20/05/2019
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10. Avaliação Microestrutural e Resistência à Corrosão de uma Junta Dissimilar entre um Aço de Alta Resistência e Baixa Liga e Aço um Inoxidável Duplex
Resumo A união entre materiais dissimilares tem sido amplamente aplicada na indústria de petróleo e gás. Em geral, este tipo de soldagem é mais sensível às diferenças de composição química existente entre os metais envolvidos. Diante dessa perspectiva, este trabalho tem por objetivo avaliar, por união autógena, a microestrutura de uma junta sold
Soldag. insp.. Publicado em: 16/05/2019
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11. Failure Probability, Stress Distribution and Fracture Analysis of Experimental Screw for Micro Conical Abutment
Resumo O objetivo deste estudo foi avaliar a probabilidade de falha de dois tipos de parafusos para pilar protético após a compressão e analisar a distribuição da tensão com o método dos elementos finitos. Sessenta (60) restaurações unitárias foram montadas em implantes de titânio (e-fix, A.S. Technology - Titanium Fix). Os grupos foram divididos
Braz. Dent. J.. Publicado em: 04/04/2019
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12. New Synthesis Method for a Core-Shell Composite Based on α-Bi2O3 @PPy and its Electrochemical Behavior as Supercapacitor Electrode
New composite based on polypyrrole (PPy) and bismuth oxide (α-Bi2O3) was investigated as supercapacitor electrode. The α-Bi2O3 was obtained by hydrothermal route at 500 ºC for 2 h. Cyclic voltammetry was used to electropolymerize PPy on graphite electrode (GE) or on GE/α-Bi2O3. The X-ray diffraction profile of Bi2O3 revealed the α-Bi2O3 monoclinic struc
J. Braz. Chem. Soc.. Publicado em: 2019-04