Recrystallization
Mostrando 1-12 de 178 artigos, teses e dissertações.
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1. Complexes with Furyl-Substituted 3-Hydroxychromone: Synthesis, Characterization and Fluorescence Studies
2-(2-Furyl)-3-hydroxychromone (HL) reacts with MII ions in the formation of quadratic [Cu(L)2] (3), octahedral [M(L)2(OH2)2] (M = Co (1), Ni (2), Zn (4), Mn (5)) and seesaw [M(L)2] (M = Sn (6), Pb (7)) complexes. Recrystallization of complexes 1-3 in presence of pyridine lead to [M(L)2(py)2] (1a-3a) aducts. All compounds were characterized by Fourier transfo
J. Braz. Chem. Soc.. Publicado em: 2021-08
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2. Antibacterial Activity of 2-Amino-1,4-naphthoquinone Derivatives against Gram-Positive and Gram-Negative Bacterial Strains and Their Interaction with Human Serum Albumin
A series of 2-amino-1,4-naphthoquinone derivatives (NQA-NQF) was synthesized by alternative methods (ultrasonication and microwave irradiation), with yields ranging from 40 to 71%, and without the need of further recrystallization. Each compound was evaluated against four Gram-positive (Bacillus subtilis, Enterococcus faecalis, Staphylococcus aureus and Baci
J. Braz. Chem. Soc.. Publicado em: 2020-09
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3. Zn2Al Layered Double Hydroxides Intercalated with Nitrate and p-Aminobenzoate as Ultraviolet Protective Agents in Low-Density Polyethylene Nanocomposites and Natural Insulating Oils
Zn2Al-Cl and Zn2Al-NO3 layered double hydroxides (LDHs) were synthesized through the fixed pH co-precipitation method and used as precursor materials for the intercalation of p-aminobenzoate through anion exchange reactions. Since chloride in Zn2Al-Cl was only partially exchanged with p-aminobenzoate, the phases Zn2Al-NO3 and Zn2Al-N -AB (nitrate exchanged w
J. Braz. Chem. Soc.. Publicado em: 2020-05
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4. Austenitic Grain Size Prediction in Hot Forging of a 20MnCr5 Steel by Numerical Simulation Using the JMAK Model for Industrial Applications
Yield strength and toughness in steels are directly associated with hot forging processes, especially by controlling austenitic grain size and cooling conditions. The phenomenological JMAK model in macroscale has been applied in different material classes to predict grain size after hot forming. However, on an industrial application, there is still a lack of
Mat. Res.. Publicado em: 05/12/2019
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5. Recrystallization Kinetics of Fe-3%Si after Deformation at High Strain Rate and High Temperature
Recrystallization kinetics of Fe-3%Si with initial grain size 296~839µm at the temperature range 1223~1423K, strain range from 0.51 to 0.92, strain rate range 5~80s−1 was studied by isothermal compression test using Gleeble-2000. The effect of strain, strain rate, initial grain size and annealing temperature on the recrystallization kinetics were discusse
Mat. Res.. Publicado em: 07/11/2019
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6. Characterization of Austenite Decomposition in Steels with Different Chemical Concepts and High Potential to Manufacture Seamed Pipes for Oil and Gas Industry
This work presents the characterization of austenite decomposition kinetics in two steels during continuous cooling considering non-deformed austenite grains. Two different chemical concepts of steels were evaluated: low carbon - high manganese and a relatively new concept based on low carbon - low manganese - high niobium contents. Dilatometric experiments,
Mat. Res.. Publicado em: 21/10/2019
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7. An Alternative to Avrami Equation
This paper proposes an alternative to the Avrami equation capable of describing whole transformation curves with significant fitting-correlations. The model bears physically meaningful parameters which permit considering the initial transformation kinetics independently from the subsequent microstructural evolution. Data of martensite, bainite, recrystalliza
Mat. Res.. Publicado em: 30/09/2019
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8. Rolling and recrystallization behavior of pure zirconium and zircaloy-4
ABSTRACT Rolling and recrystallization of pure zirconium and zircaloy-4 have been studied comparatively in this paper. For the as-received condition, zirconium presented a recrystallized microstructure and the alloy a typical basketweave microstructure. Comparative rolling tests were performed, and reduction limit curves as a function of the rolling temperat
Matéria (Rio J.). Publicado em: 16/09/2019
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9. Crystallographic texture and microtexture of copper drawn at 295 K and 77 K
ABSTRACT The pure copper wires were wiredrawn at cryogenic and room temperatures. After deformation they presented important and significant differences in their crystallographic textures and microstructures. Therefore, this study aimed to investigate the evolution of crystallographic texture of pure copper drawn at temperatures of 295 K and 77 K and correla
Matéria (Rio J.). Publicado em: 16/09/2019
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10. Improvement of Texture and Magnetic Properties in 4.5 wt.% Si Grain-Oriented Electrical Steels
4.5 wt.% Si grain-oriented electrical steel sheets were successfully produced by hot rolling, normalizing, warm rolling and annealing, and texture evolution was investigated using macro- and micro-texture analysis. It is found that the recrystallization texture of sheets is very sensitive to the warm rolling reduction, and 83-87% warm rolling reductions are
Mat. Res.. Publicado em: 19/08/2019
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11. Fabrication of Fe-2.1 wt.% Si Alloy Sheets with Dominant Goss Texture Through Thickness
Macro- and micro-texture of Fe-2.1 wt.% Si alloy sheets were investigated and analyzed by X-ray diffraction and electron backscattered diffraction techniques. A Goss ({110}<001>) component accompanied by extremely weak γ (<111>//ND, normal direction) fiber is successfully formed through the sheet thickness after primary recrystallization and considerable gr
Mat. Res.. Publicado em: 15/07/2019
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12. Double Identification of the Optimal Hot Deformation Parameter Windows for AlCu4SiMg Alloy
In order to achieve hot processing products with expected microstructures, the construction of corresponding relationships between micro-evolution mechanisms and hot processing parameters is essential. In this study, such corresponding relationships of as-cast AlCu4SiMg alloy were constructed by double evaluating processing maps and Zener-Holloman (Z) parame
Mat. Res.. Publicado em: 10/07/2019