Polycondensation
Mostrando 1-12 de 35 artigos, teses e dissertações.
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1. Assessment of Reaction Parameters in the Polymeric Carbon Nitride Thermal Synthesis and the Influence in Photocatalytic Hydrogen Production
In this work, the reaction parameters for polymeric carbon nitride synthesis by thermal polycondensation were assessed, such as type of precursor, heating rate and time of thermal treatment, in order to obtain crystalline materials with high photocatalytic performance. All synthesized materials were tested as photocatalysts in hydrogen production using ethyl
J. Braz. Chem. Soc.. Publicado em: 2020-05
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2. Effect of sawdust as porosity agent on final properties of geopolymers
Abstract The geopolymers synthesis are based on geopolymerization, a sequence of reactions processed in an alkaline medium through oligomers providing a three-dimensional molecular structure. In this work, the polycondensation of metakaolin was performed with alkaline activators (NaOH and sodium silicate), wood sawdust and other additives. Two different comp
Cerâmica. Publicado em: 2019-01
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3. Crystallization, thermal and mechanical behavior of oligosebacate plasticized poly(lactic acid) films
Abstract The biodegradable aliphatic oligoester oligo(trimethylene separate) (OTS) was synthesized by polycondensation and used to plasticize poly(lactic acid) (PLA). Casting films of PLA and PLA/OTS with concentrations of 1, 5 and 10 wt.% were prepared, and these films were characterized by thermal analyses, crystallinity, rheology and mechanical tests. DS
Polímeros. Publicado em: 29/11/2018
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4. Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
Abstract In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transform infrared spectrometer (FT-IR), nuclear magnetic
Polímeros. Publicado em: 29/11/2018
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5. Investigating the influence of conduit residues on polyurethane plates
Abstract Converting waste into a product similar to the original one or into another useful product is to save energy, protect natural resources, and bring back to the production cycle what was discarded. In that direction, new polyurethane-based composites have been developed by incorporating 5%, 10%, 15%, and 20% PVC conduit discarded by the construction i
Polímeros. Publicado em: 29/06/2017
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6. Influence of PLGA and PLGA-PEG on the dissolution profile of oxaliplatin
Abstract Oxaliplatin was inserted into polymeric matrices aiming to study the interaction of this drug with these polymers and its capability to diffuse to the environment. Tested polymers were: (1) polyethylene glycol (PEG), (2) poly(lactic-co-glycolic acid) (PLGA), and (3) a copolymer of them (PLGA-PEG). The latter two were synthesized by us using polycond
Polímeros. Publicado em: 07/06/2016
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7. Investigations on Preparation and Characterization of Certain Copolyesters
In this paper, we report on the synthesis and characterization of high molecular weight copolyesters from Terephthalic acid, 1, 4 butane diol and Succinic acid /Sebacic acid through a two step process of melt polycondensation using titanium tetra butoxide as catalyst. The synthesized aromatic-aliphatic random copolyesters were characterized by means of FTIR,
Mat. Res.. Publicado em: 26/02/2016
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8. Synthesis and characterization of novel polyester containing Schiff-base unit
Abstract A new Schiff base type of polyester containing 2,2-dimethyl-1,3-diaminopropane was prepared by solution polycondensation of 1,4-benzenedicarbonyl dichloride with Bis(4-hydroxybenzilaldehid)-2,2-dimethyl-1,3-propildiimine (H2HB2P) which is derived from a 2,2-dimethyl-1,3-diaminopropane Schiff base reacted with a 4-hydroxybenzaldehyde monomer. The mon
Polímeros. Publicado em: 2015-10
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9. Synthesis and characterization of new soluble polyamides from Acenaphtohydrazinomercaptotriazole diamine
AbstractA diamine Acenaphtohydrazinomercaptotriazole (AHTD) was synthesized in one step from acenaphthoqinone and 4-amino-3-hydrazino-5-mercapto-1,2,4-triazole. The diamin was characterized by FTIR, 1HNMR, 13CNMR and melting point. Diamin was used to prepare novel polyamides. The low temperature solution polycondensation of diamin with tow aromatic and tow a
Polímeros. Publicado em: 2015-08
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10. Polyphenolic resin synthesis: optimizing plantain peel biomass as heavy metal adsorbent
AbstractPolyphenolic resol resins were obtained from an ethanolic extraction of green plantain peels (Musa paradisiaca) grown in Colombia. A synthesis was then performed by polycondensation in an alkaline pH solution in order to perform research on phenolic resin production with high mechanical performance. The polymers were characterized by DSC and TGA anal
Polímeros. Publicado em: 2015-08
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11. Novel and Fast Microwave-Assisted Synthesis of Carbon Quantum Dots from Raw Cashew Gum
Carbon quantum dots (C-dots) with average size of 9 nm were synthesized from an aqueous solution of raw cashew gum (RCG) using a novel and fast microwave-assisted technique which involves two steps. In the first step (partial depolymerization in solution) some monomer units are formed through the autohydrolysis of CG and a small amount of 5-hydroxymethyl fur
J. Braz. Chem. Soc.. Publicado em: 2015-06
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12. Synthesis of Poly(Dimethylsiloxane) Networks Functionalized with Imidazole or Benzimidazole for Copper(II) Removal from Water
Functionalized elastomeric networks were obtained via a polycondensation reaction between poly(dimethylsiloxane) (PDMS) containing Si(CH3)2OH as end groups and an imidazole- or benzimidazole-modified alkoxysilane. The structure of the polymeric materials was characterized via attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR) and
J. Braz. Chem. Soc.. Publicado em: 2015-02