Liquid Chromatographic
Mostrando 1-12 de 668 artigos, teses e dissertações.
-
1. Innovative gas chromatographic determination of formaldehyde by miniaturized extraction and on-fiber derivatization, via SPME and SPME Arrow
Formaldehyde (FA) is a carbonyl compound, ubiquitous in the environment and among the most widespread pollutants: it has exhibited toxic properties and is classified as a human carcinogen. FA is released from several sources, both temporary (e.g., combustion processes) and permanent (e.g., building products). This work proposes an innovative fully-automated
Química Nova. Publicado em: 2022
-
2. An Online Solid Phase Extraction-Liquid Chromatography Tandem Mass Spectrometry Method for the Analysis of Parabens in Urban Waters
In this work, we report a method to quantify methylparaben, ethylparaben, propylparaben and butylparaben in urban waters of São Carlos (São Paulo State, Brazil) by online solid phase extraction-liquid chromatography tandem mass spectrometry (SPE-LC-MS/MS) system. The method achieved ng L-1 limits with good accuracy and precision (internal standards for eac
J. Braz. Chem. Soc.. Publicado em: 2021-05
-
3. Evaluation of Antibacterial Activity, Chromatographic Analysis for Rutin and Quercetin Quantification Using HPLC-UV-Vis from the Hydro-Alcoholic Extract Obtained from Bidens pilosa Linné
Novel and miniaturized technique, a dynamic sonication-assisted solvent extraction before the analysis by high performance liquid chromatography-ultraviolet visible (HPLC-UV-Vis) for isolation, identification and quantification of rutin and quercetin metabolites in alcoholic extracts from Bidens pilosa Linné, was developed. The results showed that the flowe
J. Braz. Chem. Soc.. Publicado em: 2021-03
-
4. Blue Glow Sticks: Cinnamic Acids and Arylacrylonitriles with Liquid-Crystalline Properties and Highly Fluorescent
Five new π-conjugated chromophores derived from acrylic acid and acrylonitrile were synthesized and their thermal and photophysical behaviors were analyzed. They were designed and synthesized through Knoevenagel condensations between arylacetylenebenzaldehydes and a methylene group activated from cyanoacetic and malonic acids. The characterization of the ta
J. Braz. Chem. Soc.. Publicado em: 2021-01
-
5. Novo Qualis: rumos e rumores
Pharmaceutical cocrystals are composed of a drug and a coformer and are currently gaining attention due to their possibility of improving drug solubility. Quantitative determination of cocrystals is usually carried out by liquid chromatography method, but an alternative for the same is derivative UV spectrophotometry. Cocrystals of lamotrigine (LAM) were for
Rev. Bras. Hist.. Publicado em: 2020-12
-
6. Development of a First-Order Derivative UV Spectrophotometric Method for the Assay and Solubility Evaluation of Lamotrigine and Nicotinamide Cocrystals
Pharmaceutical cocrystals are composed of a drug and a coformer and are currently gaining attention due to their possibility of improving drug solubility. Quantitative determination of cocrystals is usually carried out by liquid chromatography method, but an alternative for the same is derivative UV spectrophotometry. Cocrystals of lamotrigine (LAM) were for
J. Braz. Chem. Soc.. Publicado em: 2020-12
-
7. DETERMINATION OF THE PESTICIDES IN WATER USED IN THE CULTURE AND PROCESSING OF POTATOES
The contamination of water bodies by pesticide residues through direct flow, leaching and other methods has motivated the development of analytical methods for the determination of these compounds in water. A vortex-assisted liquid-liquid microextraction method followed by gas chromatography coupled to mass spectrometry for the determination of anilazine, li
Quím. Nova. Publicado em: 2020-09
-
8. Dereplication of Aporphine Alkaloids by UHPLC-HR-ESI-MS/MS and NMR from Duguetia lanceolata St. -Hil (Annonaceae) and Antiparasitic Activity Evaluation
Although the genus Duguetia is well known for producing alkaloids as chemical constituents, there are no reports of alkaloids identified in the species D. lanceolata. Thus, aiming to identify the chemical composition of this species, the dereplication of alkaloidic phase was performed by use of ultra-high performance liquid chromatography high resolution ele
J. Braz. Chem. Soc.. Publicado em: 2020-09
-
9. A Simple and Effective Liquid-Liquid-Liquid Microextraction Method with Ultraviolet Spectrophotometric Detection for the Determination of Bisphenol A in Aqueous Matrices and Plastic Leachates
This study shows the development and application of an analytical method for the determination of bisphenol A (BPA) in aqueous samples such as tap, river and mineral water and plastic leachates, based on an extensive literature search to understand the gaps for the determination of BPA in aqueous samples. We found that most of the methods in the literature e
J. Braz. Chem. Soc.. Publicado em: 2020-08
-
10. Systemic treatment and surgery versus systemic treatment alone for metastatic breast cancer
This study shows the development and application of an analytical method for the determination of bisphenol A (BPA) in aqueous samples such as tap, river and mineral water and plastic leachates, based on an extensive literature search to understand the gaps for the determination of BPA in aqueous samples. We found that most of the methods in the literature e
Rev. Assoc. Med. Bras.. Publicado em: 2020-08
-
11. SPECIATION ANALYSIS OF ARSENIC IN RICE USING HIGH PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED WITH HYDRIDE GENERATION ATOMIC FLUORESCENCE SPECTROMETRY (HPLC-HG-AFS)
The aim of this work was to develop a method using high performance liquid chromatography coupled with hydride generation atomic fluorescence spectrometry (HPLC-HG-AFS) for the determination and speciation analysis of the inorganic and organic species of arsenic found most often in rice samples: As(V), As(III), monomethylarsonic acid (MMA), and dimethylarsin
Quím. Nova. Publicado em: 2020-06
-
12. Methodology Development and Validation of Amphotericin B Stability by HPLC-DAD
The high worldwide consumption of antibiotics and their complex impurity profiles has drawn the attention of the scientific community to the development and validation of stability methods for these drugs. Amphotericin B is an antibiotic that is a natural fermentation product of bacterium Streptomyces nodosus, used as a broad-spectrum antifungal agent, and i
J. Braz. Chem. Soc.. Publicado em: 2020-05