Icpms
Mostrando 1-12 de 238 artigos, teses e dissertações.
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1. A química analítica aplicada aos estudos de pigmentos rupestres: uma revisão
Instrumental advances have been employed in the study of archeological remains such as prehistoric rupestrians paintings with the objective of chemically characterizing them in order to reconstruct the cultural technologies of a prehistoric human group and/or to support conservation science studies. The analytical techniques most commonly used in archaeometr
Química Nova. Publicado em: 2022
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2. Solventes eutéticos naturais profundos (NADES) no preparo de amostras de rocha fosfática e suplemento mineral para determinação elementar por técnicas de plasma
Natural deep eutectic solvents (NADES) based on xylitol, citric acid, and malic acid were synthesized and used in ultrasound-assisted extraction (UAE) and heating-bath extraction of phosphate rock and mineral supplement samples. Arsenic, Ca, Cd, Cr, Cu, Fe, K, Mg, Mn, Na, P and Zn were determined by inductively coupled plasma mass spectrometry (ICP-MS) and i
Quím. Nova. Publicado em: 2021-06
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3. Alternative Approaches Applied to Inductively Coupled Plasma Techniques: Multi-Flow and Two-Flow Calibration
Multi-flow calibration (MFC) is based on monitoring the analytical signal from a single calibration standard solution at several different nebulization gas flow rates (Q), which normalizes plasma conditions and minimizes matrix effects. In the present study, MFC was evaluated, for the first time, applied to inductively coupled plasma optical emission spectro
J. Braz. Chem. Soc.. Publicado em: 2021-04
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4. Spatial Distribution and Pollution Assessment of Trace Elements Pb, Cu, Ni, Fe and As in the Surficial Water of Staring Bay, Indonesia
Staring Bay has long been used by the local community for fisheries and fishing activities; however, the rapid population growth and industrial activities around the bay in recent years are predicted to contribute significantly to the increase of waste entering the bay. This particular study was aimed to provide baseline levels of trace elements Pb, Cu, Ni,
J. Braz. Chem. Soc.. Publicado em: 2021-02
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5. DETERMINAÇÃO DE MERCÚRIO EM FÍGADO DE TETRÁPODES MARINHOS POR ESPECTROMETRIA DE FLUORESCÊNCIA ATÔMICA ACOPLADA A GERAÇÃO DE VAPOR FRIO (CV-AFS) E ESPECTROMETRIA DE MASSA COM FONTE DE PLASMA INDUTIVAMENTE ACOPLADO (ICP-MS): UMA COMPARAÇÃO SISTEMÁTICA ENTRE AS DUAS TÉCNICAS
This study compares the techniques cold vapour atomic fluorescence spectrometry (CV-AFS) and inductively coupled plasma mass spectrometry (ICP-MS) for the determination of Hg in biological samples (hepatic tissue from marine tetrapods). Acid digestions were performed for the samples and aliquots of them were analysed by ICP-MS and CV-AFS. To minimize the Hg
Quím. Nova. Publicado em: 2021-01
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6. Arsenic and Other Elements Determination in Seawater Using Coprecipitation and Standard Mode Inductively Coupled Plasma Mass Spectrometry
The present work aims the determination of As, Co, Cr, Cu, Mn and Pb in seawater samples using coprecipitation extraction procedure before standard mode inductively coupled plasma mass spectrometry (ICP-MS) (no collision/reaction cell). The coprecipitation procedure is based on the precipitation of Mg(OH)2 from the reaction of the Mg2+ ions (present into the
J. Braz. Chem. Soc.. Publicado em: 2021-01
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7. Study of Inorganic Profiles of Street Cocaine Samples Using ICP-MS and ICP OES
Determining inorganic constituents in illicit drugs can indicate its purity and presence of adulterants. In this study, we analyzed 52 street cocaine samples, seized in three different regions of Espírito Santo, state of Brazil. Inductively coupled plasma optical emission spectrometry was used to determine Al, Ca, Cu, Fe, Mn, Mg, Zn concentrations and induc
J. Braz. Chem. Soc.. Publicado em: 2021-01
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8. “Half-Sandwich”/RuII Anticancer Complexes Containing Triphenylphosphine and p-Substituted Benzoic Acids
Mononuclear and binuclear RuII/arene/triphenylphosphine complexes with p-substituted benzoic acid derivatives were prepared and characterized. These monocationic complexes of type [Ru(η6-p-cymene)(PPh3)L] (L = benzoic acid (1), p-hydroxybenzoic acid (2), p-nitrobenzoic acid (3) and terephthalic acid (4)) were characterized using various techniques, such as
J. Braz. Chem. Soc.. Publicado em: 2020-11
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9. Quantification of Arsenic, Cadmium, Mercury and Lead in Pineapple: Method Development, Validation and Evaluation of In-House Reference Materials
A method for quantification of arsenic, cadmium, mercury, and lead in pineapple using inductively coupled plasma-mass spectrometry (ICP-MS) was developed, validated, and used to test the homogeneity and stability of in-house reference materials. The method was tested at the regulation levels given by the Food and Agriculture Organization of the United Nation
J. Braz. Chem. Soc.. Publicado em: 2020-06
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10. Selenium biofortification on garlic growth and other nutrients accumulation
RESUMO O selênio (Se) é elemento essencial para os seres humanos e é considerado anticancerígeno. Alho pode acumular Se, sendo, por isso, uma opção para a suplementação de Se na dieta humana. Assim, o objetivo deste trabalho foi estudar a captação e acúmulo de selênio durante o crescimento do alho e avaliar os efeitos da fortificação de Se. Qua
Hortic. Bras.. Publicado em: 07/11/2019
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11. Corrosion Resistance of Stainless Steel Brackets After Thermal Recycling by Direct Flaming
Abstract Objective: To determine and compare the corrosion resistance (based on the release of nickel and chromium in artificial saliva) of various brands of stainless steel brackets after thermal recycling by direct flaming. Material and Methods: This research study employed 40 stainless-steel maxillary premolar brackets from different brands (Ormco, GAC,
Pesqui. Bras. Odontopediatria Clín. Integr.. Publicado em: 31/10/2019
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12. Nanostructured Systems Obtention Using LbL Self-Assembly or the Cysteine-Assisted Adsorption Method and Their Application as a Water Splitting Single Catalyst
The present work evaluated the effect on charge transfer in functionalized TiO2 nanostructured systems using different binders. We highlight the conditions required to form self-assembled systems by varying the number of layers, as well as by substituting them for an organic binder, cysteine. Additionally, we study the pH effect of the precursor solution (HA
J. Braz. Chem. Soc.. Publicado em: 24/10/2019