Direct Analysis Method
Mostrando 1-12 de 803 artigos, teses e dissertações.
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1. Determination of Ethyl Carbamate in Commercial Sweetened Sugar Cane Spirit by ESI-MS/MS Using Modified QuEChERS and 18-Crown-6/Trifluoroacetic Acid Spiking Additives
A fast, sensitive, and selective direct injection electrospray tandem mass spectrometry (DI ESI MS/MS) method that is able to quantify ethyl carbamate in commercial sweetened sugar cane spirit is described. The preparation method uses a modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) with potassium carbonate added to sweetened sugar cane
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Validation of the single-platform ISHAGE protocol for enumeration of CD34+ hematopoietic stem cells in umbilical cord blood in a Brazilian center
Abstract Background This study aims to validate the single-platform method for enumeration of CD34+ cells, by comparing the performance of two different commercial kits, as well as to evaluate the efficiency of the AccuriTM C6 cytometer in providing direct counts of absolute cell numbers. Method We evaluated 20 samples from umbilical cord blood (UCB), comp
Hematology, Transfusion and Cell Therapy. Publicado em: 2022
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3. HDL-Cholesterol in Children and Adolescents with Congenital Heart Disease
Abstract Background Children and adolescents with congenital heart disease may be more likely to develop atherogenic cardiovascular diseases in adulthood. Therefore, the early identification of risk factors and intervention in childhood may be crucial for a good quality of life and longevity. Objectives To describe the distribution of high-density lipoprot
International Journal of Cardiovascular Sciences. Publicado em: 2022
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4. Finite strip method computer application for buckling analysis of thin-walled structures with arbitrary cross-sections
Abstract The Direct Strength Method (DSM) is a well-known formulation presented in the Brazilian standard ABNT NBR 14762:2010, that estimates the strength capacity of cold-formed steel (CFS) members. However, this formulation requires the elastic critical buckling loads as point of departure, regarding local (L), distortional (D) and global (G) modes, which
REM, Int. Eng. J.. Publicado em: 2021-09
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5. Development of a Simple and Fast Procedure Based on Acid Dilution for Determination of Macro and Microelements in Guarana-Based Beverages by ICP OES
A simple analytical procedure is proposed for the direct analysis of guarana-based beverages in order to determine nutrient elements by inductively coupled plasma optical emission spectrometry (ICP OES). A Box-Behnken design, combined with Derringer’s desirability function, was applied to the simultaneous optimization of the ICP OES radiofrequency (RF), sa
J. Braz. Chem. Soc.. Publicado em: 2021-07
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6. Reliability assessment of cold-formed steel beams by the FORM method
Abstract This article presents a procedure for the reliability assessment of cold-formed steel beams based on the Direct Strength Method (DSM) and the Effective Section Method (ESM). Using a comprehensive database, a statistical analysis of the test results was performed to determine the statistical properties of the professional factor random variable. The
REM, Int. Eng. J.. Publicado em: 2021-06
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7. Effect of pH level and calcination on the production of calcium phosphates by acidic route of wet precipitation
Abstract Multiphasic calcium phosphate powders were synthesized by the acidic route, using lactic acid as a chelating agent that allows the production of a stable and rich solution of calcium and phosphate ions at room temperature. After pH adjusting, without varying the concentrations of precursor solution, XRD and FTIR analyses showed different CaP phases
Cerâmica. Publicado em: 2021-06
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8. DETERMINAÇÃO DE FÓSFORO EM PALEOSSEDIMENTOS EMPREGANDO ESPECTROMETRIA DE FLUORESCÊNCIA DE RAIOS-X PORTÁTIL
Phosphorus (P) is an important chemical marker of the past human presence, because, besides indicates the localization of possible archaeological sites, also, contributes to clarify doubts regarding to origin, duration and to specific functions that were developed in them. The present study aimed to obtain a simple, accurate, fast and non-destructible analyt
Quím. Nova. Publicado em: 2021-02
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9. Direct Solid Sample Analysis of Medicinal Herbs for Determination of Ba, Cu, Ni, V and Zn by EDXRF
In this work, an analytical method for determination of Ba, Cu, Ni, V, and Zn, in medicinal herbs, through direct solid sample analysis by energy dispersive X-ray fluorescence spectrometry (EDXRF), was applied. Accuracy and precision (intra and inter day) of the analytical method were confirmed through analysis of certified reference material, tomato leaves
J. Braz. Chem. Soc.. Publicado em: 2021-01
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10. What to Expect for the New Year?
In this work, an analytical method for determination of Ba, Cu, Ni, V, and Zn, in medicinal herbs, through direct solid sample analysis by energy dispersive X-ray fluorescence spectrometry (EDXRF), was applied. Accuracy and precision (intra and inter day) of the analytical method were confirmed through analysis of certified reference material, tomato leaves
J. Braz. Chem. Soc.. Publicado em: 2021-01
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11. Lowering costs for large-scale screening in psychosis: a systematic review and meta-analysis of performance and value of information for speech-based psychiatric evaluation
Objective: Obstacles for computational tools in psychiatry include gathering robust evidence and keeping implementation costs reasonable. We report a systematic review of automated speech evaluation for the psychosis spectrum and analyze the value of information for a screening program in a healthcare system with a limited number of psychiatrists (Maputo, M
Braz. J. Psychiatry. Publicado em: 2020-12
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12. Electroanalytical Method for Determination of Trace Metals in Struvite Using Electrochemically Treated Screen-Printed Gold Electrodes
We present an electroanalytical method using square-wave anodic stripping voltammetry on electrochemically-treated screen-printed gold electrodes to the simultaneous determination of lead(II), copper(II) and mercury(II) in struvite (natural fertilizer produced from urine). Electrochemical treatment via cyclic voltammetry of the working electrodes increased s
J. Braz. Chem. Soc.. Publicado em: 2020-09