Application of a 33 Box-Behnken Design to Optimize the Extraction of Eleven Fluoroquinolones from Poultry Muscle and Kidney Using a QuEChERS Approach via Liquid Chromatography Tandem Mass Spectrometry: the Easy Use of Microsoft Excel® in Multivariate Analysis

AUTOR(ES)

Rocha, Diego G., Santos, Flavio A., Augusti, Rodinei, Faria, Adriana F.

FONTE

J. Braz. Chem. Soc.

DATA DE PUBLICAÇÃO

2016-01

RESUMO

This work presents an optimization of a quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction approach of eleven fluoroquinolones in poultry muscle and kidney using a 33 Box-Behnken factorial design. All the data treatment was performed using Microsoft Excel® 2010. The suitability of the developed method was confirmed by two proficiency tests for ciprofloxacin and enrofloxacin.

Documentos Relacionados

• Determination of Pesticides in Grape Juices by QuEChERS and Liquid Chromatography-Tandem Mass Spectrometry
• Determination of Antibiotics Residues in Milk Using a QuEChERS Method Using Full Factorial Design and Liquid Chromatography-Tandem Mass Spectrometry
• Evaluation of QuEChERS Sample Preparation and Gas Chromatography Coupled to Mass Spectrometry for the Determination of Pesticide Residues in Grapes
• Determination of pesticide residues in sugarcane honey by QuEChERS, and liquid chromatography
• Box–Behnken experimental design for extraction of artemisinin from Artemisia annua and validation of the assay method